OPTIMIZATION OF SYNTHESIS PARAMETERS FOR LEAD OXIDE NANOPARTICLES USING RESPONSE SURFACE METHODOLOGY

İsmail Kutlugün AKBAY; Ahmet GÜNGÖR; Rükan GENÇ; Tonguç ÖZDEMİR

OPTIMIZATION OF SYNTHESIS PARAMETERS FOR LEAD OXIDE NANOPARTICLES USING RESPONSE SURFACE METHODOLOGY

İsmail Kutlugün AKBAY, Ahmet GÜNGÖR, Rükan GENÇ, Tonguç ÖZDEMİR

Öz

Nano-sized lead oxide has useful applications that can be used in industrial production. In this study, the synthesis parameters were optimized using response surface methodology and also ANOVA study were done. Reaction temperature, sodium hydroxide and lead II acetate concentration were studied. The modification was lead to increase adequate precision of model. Close results between R₂ and R_2adjshowed the accuracy of model. The optimum results of the study were found 14.89 M NaOH concentration, 0.87 M Pb(II)Ac and reaction temperature of 88.56 °C. Under optimum parameters, the particle size of lead II oxide was found to be 19.75 nm.

Anahtar Kelimeler

Nanoparticle; RSM; Optimization; Lead Oxide; Central Composite Design

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Referanslar

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